| Column (HP-5) | 30 m length × 0.25 mm i.d. × 0.1 μL film thickness |
| Detector | Flame ionization detector (FID) |
| 5973 mass selective detector (MSD) |
| Carrier gas | Helium |
| Injector type | Splitless mode |
| Purge time | 45 min |
| Purge flow | 15 mL/min |
| Flow rate | 1 mL/min |
| Inlet temperature | 250℃ |
| Detector temperature | 270℃ in FID |
| Oven temperature | Initial temp : 40℃ |
| Initial holding time : 5 min |
| Rate : 4℃/min until 160℃ |
| Rate : 10℃/min until 250℃ |
| Final temp : 250℃ |
| Final holding time : 6 min |
|
| 5973 mass selective detector |
|
| Ion source temperature | 178℃ |
| Ionization energy | 70 eV |
| Scan | 2.0 Scans/s |
| Filament emission | 1 mA |
| Library | Wiley 77n MS library |