Table 3. Precision and accuracy data for the determination of natural food preservatives in spiked cheese
Compound | Spiked concentration (μg/mL) | Detected concentration (μg/mL) | Recovery (%) | Intra-day test (n=3, RSD%) | Inter-day test (n=9, RSD%) |
Benzoic acid | 4.00 | 3.81±0.08 | 95.35±1.99 | 2.09 | 3.19 |
2.00 | 1.97±0.04 | 98.60±1.79 | 1.82 | 1.97 |
1.00 | 1.00±0.04 | 99.83±3.99 | 4.02 | 2.66 |
Sorbic acid | 5.00 | 5.06±0.04 | 101.14±0.80 | 0.78 | 3.46 |
2.50 | 2.55±0.15 | 101.96±4.64 | 4.44 | 6.26 |
1.25 | 1.27±0.07 | 97.84±5.03 | 3.77 | 7.78 |
Propionic acid | 40.00 | 37.12±0.82 | 92.80±2.04 | 2.28 | 3.60 |
20.00 | 19.24±0.79 | 96.22±3.97 | 4.43 | 6.39 |
10.00 | 9.96±0.46 | 99.56±3.75 | 5.31 | 5.78 |
Nitrate | 10.00 | 9.43±1.63 | 94.27±1.04 | 1.12 | 9.53 |
5.00 | 4.78±0.86 | 95.22±1.89 | 2.00 | 8.89 |
2.50 | 2.51±0.45 | 95.07±4.58 | 5.29 | 3.60 |