Table 1. Specification and operating condition of GC for propionic acid analysis

Device Parameter Condition
GC Column HP-FFAP (0.32 mm i.d.×30 m, 0.25 μM)
Oven temperature program 60°C (4 min) → 115°C (28°C/min) → 240°C (20°C/min, 5 min)
Inlet temperature 200°C
Injector temperature 200°C
Injection volume 1 μL
Split ratio Splitless
Carrier Helium, 1.0 mL/min
MS Ionization mode EI
Electron impact mode 70 eV
Selected ion (m/z) 741), 57, 45
MS ion source temperature 200°C
Quantitation ion.
GC, gas chromatograph; MS, mass spectrometer.