Table 5. Validation of other livestock and fishery products using Method 1

Matrix	Target	Linearity (r2)	Fortification (μg/kg)	Recovery (%)	CV (%)	LOD (μg/kg)	LOQ (μg/kg)
Beef	Flunixin	0.9952	10	93.1	6.9	8	27
			20	82.4	7.7
			40	88.4	2.3
	5-Hydroxy flunixin	0.9928	10	83.3	20	10	33
			20	93.0	16
			40	100	18
Chicken	Flunixin	0.9981	5	97.5	8.9	2	7
			10	90.6	1.7
			20	99.1	4.5
	5-Hydroxy flunixin	0.9904	5	100	9.7	5	16
			10	88.4	4.5
			20	88.0	8.4
Egg	Flunixin	0.9992	5	104	1.2	3	8
			10	103	4.5
			20	108	2.8
	5-Hydroxy flunixin	0.9955	5	104	6.8	3	11
			10	102	8.1
			20	103	2.2
Flatfish	Flunixin	0.9984	5	105	7.9	2	5
			10	110	2.4
			20	96.6	2.4
	5-Hydroxy flunixin	0.9989	5	98.7	8.3	2	6
			10	96.1	4.8
			20	95.6	7.1
Shrimp	Flunixin	0.9967	5	106	5.5	2	6
			10	107	6.5
			20	99.5	7.2
	5-Hydroxy flunixin	0.9989	5	101	7.2	2	7
			10	106	7.7
			20	92.8	8.5

CV, coefficient of variation; LOD, limits of detection; LOQ, limits of quantification.